| ชื่อเรื่อง | : | Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3 |
| นักวิจัย | : | Liu, L. , Warrener, Ronald Norman. , Tiekink, E. R. T. , Russell, R. A. |
| คำค้น | : | TBA , TBA , TBA , Chemical processes. , Molecular structure. |
| หน่วยงาน | : | Central Queensland University, Australia |
| ผู้ร่วมงาน | : | - |
| ปีพิมพ์ | : | 2545 |
| อ้างอิง | : | http://hdl.cqu.edu.au/10018/4914 , cqu:2211 |
| ที่มา | : | Lui, L, Warrener, R, Russell, R & Tiekink, E 2002, 'Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3', Zeitschrift fur Kristallographie -New Crystal Structures, vol. 217, no. 4, pp. 585-586. |
| ความเชี่ยวชาญ | : | - |
| ความสัมพันธ์ | : | Zeitschrift fur kristallographie - new crystal structures Munich, Germany : R Oldenbourg Verlag, 2002. Vol. 217, no. 4, p. 585-586 2 pages Refereed 1433-7266 , aCQUIRe [electronic resource] : Central Queensland University Institutional Repository. |
| ขอบเขตของเนื้อหา | : | - |
| บทคัดย่อ/คำอธิบาย | : | C18H19NO3, monoclinic, P121/n1 (No. 14), a+8.454(6) A, b=13.123(3) A, c=14.698(3)A,P=104.85(3)o, V=1576.2 A3, Z=4, Rgt(F)=0.062, wRref(F2)=0.184, T=293 K. Source of material. This compound was prepared by the method described in the previous paper [1] but replacing the 3,4-dihydroisoquinoline with N(2'-methoxyethyl)-bezaldimine (0.815 g, 5mmol). Following chromatography, the product was isolated and recrystallised from ethanol in 13% yield (mp 407 K - 407.5 K). The product was characterised by a 3J coupling between the cis-related protons H-3 and H-4 of 6.9 Hz[2]. Experimental details The H atoms were placed in their geometrically calculated positions and included in the final refinement in the riding model approximation. |
| บรรณานุกรม | : |
Liu, L. , Warrener, Ronald Norman. , Tiekink, E. R. T. , Russell, R. A. . (2545). Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3.
กรุงเทพมหานคร : Central Queensland University, Australia. Liu, L. , Warrener, Ronald Norman. , Tiekink, E. R. T. , Russell, R. A. . 2545. "Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3".
กรุงเทพมหานคร : Central Queensland University, Australia. Liu, L. , Warrener, Ronald Norman. , Tiekink, E. R. T. , Russell, R. A. . "Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3."
กรุงเทพมหานคร : Central Queensland University, Australia, 2545. Print. Liu, L. , Warrener, Ronald Norman. , Tiekink, E. R. T. , Russell, R. A. . Crystal structure of (3s*,4s*)-4-hydroxy-2-(2'methoxyethyl)-3-phenyl-3-4-dihydroisoquinol-1(2h)-one, c18h19no3. กรุงเทพมหานคร : Central Queensland University, Australia; 2545.
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