Utilization of organic waste by transformation of several kinds of leaves and petioles waste residue and food waste into renewable energy required anaerobic digestion technology both single and two-stage digestion. In this work, it focused on sequencing batch digester called paired reactor in order to obtain the highest methane yield. It was performed during October 2012 to September 2013 by design and experiment using the low rate reactor size 20 l and feed at F/M ratio 0.15 for 2 times per set of experiment. The total set of this experiment was 4 sets. It was found that the sequencing batch digester of the 1st set of experiment produced the quantity of biogas (61.1 l/13 days) more than that of the same type of digester of the 2nd set of experiment (31.3 l/13 days) that only food waste was fermented. As for the single digester of the 3rd set of experiment, it also produced the quantity of biogas (127.5 l/13 days) more than that of the same type of digester of the 4th set of experiment (89.4 l/13 days) that only food waste was also fermented. The average quantity of methane yield in the sequencing batch digester of the 1st set of experiment (64.4 %) was more than that of the 2nd set of experiment (41.8 %). In addition, the average quantity of methane yield in the single batch digester of the 3rd set of experiment (54.65 %) was more than that of the 4th set of experiment (17.7 %). Moreover, the efficiency of organic removal in terms of COD of the 1st set of experiment (46.67 %) was higher than that of the 2nd set of experiment (29.87 %). This COD removal efficiency of the single digester of the 3rd set of experiment (64.65 %) was also higher than that of the 4th set of experiment (52.53 %). According to this difference of biodegradable in terms of the % COD removal efficiency, it is recommended to calculate this efficiency value by determination of BOD, as well as, improving the ratio of waste residue and F/M ratio in further study.